40m QIL Cryo_Lab CTN SUS_Lab TCS_Lab OMC_Lab CRIME_Lab FEA ENG_Labs OptContFac Mariner WBEEShop
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ID Date Author Type Category Subject
  2647   Thu Aug 19 14:34:10 2021 RadhikaDailyProgressCryo vacuum chamberCooldown model fitting for MS

Building on [2643], I realized that the conductive cooling term proportional to (T_{coldplate} - T_{testmass}) was also negligible. I added back in physical parameters for the 2 radiative terms (one from the cold plate, one from 295K) and used the emissivities of the test mass and inner shield as fit parameters:

F_e = (\frac{1}{e_{tm}} + (\frac{1}{e_{is}} - 1) \frac{A_{testmass}}{A_{innershield}})^{-1}

P_{rad} = F_e A_{testmass} \sigma (T_{coldplate}^4 - T_{testmass}^4)

F_{e295} = (\frac{1}{e_{tm}} + (\frac{1}{e_{is}} - 1) \frac{A_{testmass}}{A_{aperture}})^{-1}

P_{rad295} = F_{e295} A_{testmass} \sigma (295^4 - T_{testmass}^4)

I used Koji’s input to model radiative heating from 295K. I approximated the radius of the aperture (from which room temperature could be exposed) to be 3cm, and assumed radiative heat is emitted from this circle. 

The result of this fit can be seen in Attachment 1: [e_testmass, e_innershield] = [0.59736291, 0.20177643]. This would imply that Aquadag has an emissivity of about 0.6, and that the emissivity of rough aluminum is much higher than expected at 0.2.

I then used these parameters to model the cooldown, given: 1. both the test mass and inner shield surfaces are painted in Aquadag; 2. only the inner shield surface is painted in Aquadag. These models are shown in Attachment 2. 

Painting the inner shield in addition to the test mass would yield marginal improvement, as expected. However, painting the inner shield while removing Aquadag from the test mass would, according to this model, weaken the coupling further compared to the reverse case. This makes sense, since in Fe the effect of the inner shield’s emissivity is scaled by the ratio \frac{A_{testmass}}{A_{innershield}}, which is quite small. Increasing the emissivity of the test mass therefore makes more of a difference in the coupling. 

  2646   Wed Aug 18 13:06:03 2021 Aidan, StephenLab InfrastructureCleanlinessNorth table clean-up

Stephen and I spent about an hour today tidying up the North Table in preparation for 2um photodiode testing in the Megastat.

Decepticon - Transformers Wiki

I ordered two more wire racks (24" deep, 36" wide, 27" high with two shelves each) to go under the table and serve as instrumentation racks.

  2645   Sun Aug 15 00:33:15 2021 KojiSummaryCryo vacuum chamberAquadag painting on the inner shield

[Stephen Koji]

We applied Aquadag painting on the inner side of the inner shield.

  • Upon the painting work, we discussed which surfaces to be painted. Basically, the surface treatment needs to be determined not by the objects but by the thermal link between the objects.
    • We want to maximize the heat extraction from the test mass. This means that we want to maximize the emissivity factor between the test mass and the inner shield.
    • Therefore the inner barrel surface of the inner shield was decided to be painted. The test mass was painted in the previous test.
    • For the same reason, the lid of the inner shield was painted.
    • It is better to paint the cold plate (table) too. But we were afraid of making it too messy. We decided to place the painted Al foil pieces on the table.
       
    • The outer surface of the inner shield and the inner surface of the outer shield: Our outer shield is sort of isolated from the cold head and the steady-state temp is ~240K. Therefore we believe that what we want is isolation between the inner and outer shields. Therefore we didn't paint these surfaces. (note that in Mariner and beyond, the outer shield will be cooled, not isolated, and the radiative link to the outer shield would be strong by design)
    • I believe that this is not the ideal condition for the inner shield. We need to model the cryo stat heat load and take a balance between the isolation and the conduction between the outer shield and the cold head so that we gain the benefit of the outer shield as a "not so hot" enclosure.
       
  • OK, so we painted the inner barrel of the inner shield, the lid of the inner shield, and some Al foils (shiny side).
  • Stephen made the Aquadag solution. The solution was 2 scoops of Aquadag concentrate + 6 scoops of water, and the adhesion/runniness test was done on a piece of aluminum foil.
  • The barrel and the lid were painted twice. Attachment 1 shows the painting of the inner shield cylinder. Attachment 2 shows a typical blemish which necessitates the second coat.
  • To accelerate the drying process, we brought the heat gun from the EE shop --> (update - returned to EE shop, see Attachment 3)
     
  • We took some photos of the process. They are all dumped in the QIL Cryo Vacuum Chamber Photo Dump album in the ligo.wbridge account.
  2644   Fri Aug 13 21:01:42 2021 RadhikaDailyProgressCryo vacuum chamberCooldown model fitting for MS

Wow, nice fit!

How is this c compared to the 300K exposure from the open aperture for the oplev beam?
We tried to cover all the ports but one. A naive assumption is that we have this opening with this aperture size, but the heat leakage could be more than that.
e.g. the aperture allows angled infrared to come into the chamber and the inner shield reflects the hot radiation inside (and a part of it reaches the test mass).

  2643   Fri Aug 13 15:14:14 2021 RadhikaDailyProgressCryo vacuum chamberCooldown model fitting for MS

Per Koji's suggestion, I added two terms to the expression for test mass cooling power for radiative/conductive cooling from 295K (see 2641):

P_{radiative,295K} = {\color{Green} c} \sigma (295^4 - T_{testmass}^4);  P_{conductive,295K} = {\color{Green} d} (295 - T_{testmass}).

I added 0 as a lower bound for fitting a, b, c, and d. The best fit for d came out to be neglible (on the order of 10-17): conductive heating from room temperature can be ignored. The best-fit parameters for [a, b, c] came out to:  [0.025, 0.003, 0.001]. The result can be seen in Attachment 1. 

This fit would imply that there is some radiative heating of the test mass from room temperature, in addition to expected radiative/conductive cooling from the inner shield / coldplate. It is worth investigating what might be causing this, and if nothing can be determined then the model needs to be revisited. 

Quote:

How about incorporating radiative and conductive terms from the object at 300K?

 

 

  2642   Wed Aug 11 18:00:19 2021 KojiDailyProgressCryo vacuum chamberCooldown model fitting for MS

How about incorporating radiative and conductive terms from the object at 300K?

 

  2641   Wed Aug 11 14:58:47 2021 RadhikaDailyProgressCryo vacuum chamberCooldown model fitting for MS

I've made simplifications to the testmass cooling model. Assuming 2 possible cooling mechanisms, radiative and conductive, the ODE must be a function of only (T_{coldplate}^4 - T_{testmass}^4) and (T_{coldplate} - T_{testmass}). If conductive cooling/heating of the testmass is treated as negligible, as we previously assumed, then:

\ddot{Q}_{testmass} \approx {\color{Blue} a} \sigma (T_{coldplate}^4 - T_{testmass}^4), where a is the fit parameter. I include \sigma in the equation because it would appear as a constant in any radiative transfer model. I use the measured coldplate/inner shield temperature data for T_{coldplate}. Note that \frac{dT}{dt} = \frac{\ddot{Q}}{Cp*m}, and here and throughout I use a temperature-dependent Cp_{Si}(T).

The best fit parameter is a = 0.014, and the result of this fit can be seen in Attachment 1. The disagreement between the best-fit model and data suggest that cooling is not only dependent on (T_{coldplate}^4 - T_{testmass}^4), i.e. it cannot be radiative alone. I added back a conductive heating/cooling component:

\ddot{Q}_{testmass} = {\color{Red} a} \sigma (T_{coldplate}^4 - T_{testmass}^4) + {\color{Red} b}(T_{coldplate} - T_{testmass}), where a and b are the parameters of the fit. 

The result of the fit can be seen in Attachment 2. The best fit parameters [a, b] = [0.022, -0.0042]. This model matches the data much better than the purely radiative model, but the negative sign on b is non-physical (I think) since (T_{coldplate} - T_{testmass}) should always be < 0, so the sign of the conductive term should also be < 0. I'm not sure how to interpret this result, but it almost seems like there is conductive heating to the test mass even though physically this shouldn't be the case. 

  2640   Fri Aug 6 16:15:03 2021 PacoLab Infrastructure2micronLasersBrimrose AOM and amplifier

Also borrowed Mini-Circuits amplifier ZFL-500LN+ from same setup.

Quote:

Yesterday I came in the QIL and performed an express kidnapping of the 2um in fiber AOM (Brimrose) and the 5 W RF amplifier that was hooked to the RF in port (though it seems it saturates at ~ 600 mW from past elogs). I will test it with the 1419 nm ECDL fiber pickoff port to see that it works and if it doesn't I will reinstall it in the 2um testing facility.

 

  2639   Thu Aug 5 14:29:42 2021 StephenLaser2um PhotodiodesOptical design for 2um PD in new cryo chamber

Actions on my to-do list, once we are warm and up to air, before Aidan and I are able to run the JPL PD test. This list complements the optical setup tasks and data acquisition setup tasks that are also mentioned by Aidan in this thread.

Update 23 August - using this list to [comment on details] and highlight items which are still outstanding instead of duplicating in a daily progress log entry :)

0. Remove Aaron and Shruti’s Si cantilever clamp, and return to them for safekeeping [I set the clamp aside, need to coordinate return of cantilever to with Aaron!]
1. Solder a connector equivalent to the testpiece (ref. QIL/2465) but with the cryo wire, In-Ag solder on the connector end, and crimped plug pins on the free end. The crimped plug pins interface the with receptacle pins of the existing leads, which are connected to in-vac side of DB9 feedthrough).
 - need to locate some In-Ag solder! [done, and checked connectivity - used standard lead-tin solder following Rana's recommendation (ref. QIL/2418) born out by Koji's testing (ref. QIL/2462 and QIL/2465)]
2. Confirm which PD holder will be most useful for this effort (Koji’s newly machined holders might be useful?) and mount to cold baseplate. If using the tombstone from the IRLabs dewar, which is likely shorter than the beam height, it sounds like we would need to mount it on a pedestal or post. [Aidan used Koji's taller PD mount from the same purchase (ref. QIL/2459). The beam height required no modification, nice!]
3. Mount RTD to PD holder, likely with cryovarnish (unless there is a lucky extra hole for a screw/clamping post). [Radhika and Aidan's G2100807 demo shows the problem with the prior lug, not super stable mounting for the RTD as the same hole is being used to host two screws. Instead, I retrofitted the upper screw from the mount's retaining ring to host one of the trusty spring clamps, see Attachment 1. I checked for clipping or connector interference throughout, and found none.]
4. Mount heater to ___ (TBD, ideally on PD holder but possibly on cold baseplate nearby). [dog-clamped the heater to the baseplate, directly adjacent to the mount - see overview images in Attachment 2 and Attachment 3. We may go through some PID growing pains with this configuration, and we also need to learn whether the 22 W heater power locally applied can overcome the cryocooler's  ~50 W cooling power at our operating temperatures (ref. Radhika's QIL/2585). Might be necessary to intermittently power cycle the cryocooler.]
5. Confirm alignment of shields and PD. [aligned both shields, clamped inner shield, but could reposition if there is an issue.]
6. Verify electrical continuity of PD cable, RTDs, and heater. [note need to add indium and finalize clamping of PD holder, also note routing of pins to be connected to PD connector per Koji's QIL/2605 as described in Attachment 3]
7. Close up (shield lids, chamber lid). [note that in particular, the covering up (with foil sheets) of unused shield apertures is still WIP but wasn't originally mentioned!]
8. (anytime, optional) complete RTD and Heater disconnection junctions with in-vac crimped pins. [done, with mounting isolation achieved by kapton tape as ptfe tubing has not yet arrived. Attachment 4 shows one example, from the inner shield.]
 - crimped plug pins were in 40m lab parts tower, but didn’t see any receptacle pins in the vicinity. [ordered a few hundred new socket pins, I should share some with the 40m parts tower]

Pending Aaron and Shruti’s measurements, it is likely that heater-assisted warmup will occur starting Tuesday, in time for Wednesday/Thursday access. Friday 13th August could be the start of the cool down if everything goes to plan. [Nothing goes well on Friday the 13th. Aaron and Shruti do not need in-vacuum measurements anytime soon. The current plan is for cooldown to begin Tuesday and, if everything goes to plan, we will collect data through the week, then likely swap out the PDs on Monday for another run next week. The next experiment slated for the QIL Vacuum Cryostat is another Si mass radiative cooling run w/ black paint on inner surfaces of inner shield.]
 

  2638   Thu Aug 5 14:12:36 2021 StephenDailyProgressCryo vacuum chamberloading cantilevers into megastat (and actions toward pumping down)

Actions on my to-do list, before we are able to pump down for Aaron and Shruti’s Si Cantilever Q measurement:

0. Confirm Aaron has completed cantilever mounting and is happy with shield alignment.
 - if needed, might have to rotate shields and/or clamp down workpiece holder.
[Done 2021.08.07] 1. Solder on new RTD, then mount RTD and heater to workpiece holder.
2. Verify electrical continuity of RTDs and heater.
3. Close up (shield lids, chamber lids).
4. (anytime, optional) complete RTD and Heater disconnection junctions with in-vac crimped pins.
[Koji indicated these were likely scavanged from DB connector kits, Stephen ordered more] - crimped plug pins were in 40m lab parts tower, but didn’t see any receptacle pins in the vicinity.

[update - Aaron indicated interest in deferring 1 week to establish more permanent setup. Likely to reattach outer shield RTD to cantilever clamp, allowing two different workpiece sensors] Planning to complete items on this list Friday, by Mariner meeting timeslot at the latest.We are in good shape to pump down Friday early afternoon, and for Aaron to collect data via controlled warmup on Monday/Tuesday (could run through Wednesday, if needed).  

  2637   Thu Aug 5 12:39:56 2021 AidanLaser2um PhotodiodesOptical design for 2um PD in new cryo chamber

Here's a more detailed layout of the in-air design for the PD testing. Things to note:

  1. I've changed the telescope to a ~1:2 beam expander using a 40mm lens and a 75mm lens. This allows for greater tuning of the beam size on the PD
  2. I added the picomotor mirror for fine-tuning of the beam steering onto the PD (I have to check how much control this translates to on the PD inside the vacuum system).
  3. The picomotor mirror is open loop, so there is a QPD to monitor the actual pointing of the mirror
Quote:

I've sketched out a way to change the beam size on the in-vacuum PD. I think the beam diameter coming from the collimator is 1.2mm, but I need to check this. If we add a telescope outside the vacuum system and put the second lens of this on a translation stage, then this provides us with wide control of the beam size on the PD inside the vacuum system (about 400mm away).

 

 

 

 

  2636   Thu Aug 5 11:53:26 2021 RadhikaDailyProgressCryo vacuum chamberCooldown model fitting for MS

I've used the following model for cooling of the coldplate and testmass in Megastat:

P_{coldplate} = c \frac{\kappa A}{l}(T_{coldhead} - T_{coldplate}) + F_e(bp, cp) A_{coldplate} \sigma (T_{baseplate}^4 - T_{coldplate}^4),

where F_e(bp, cp) = \frac{e_{bp} e_{cp}}{e_{bp} + e_{cp} - e_{bp}e_{cp}}, and e_cp and e_bp are the emissivities of the coldplate and baseplate, respectively. The first term is conductive cooling of the cold plate via copper braid, and the second term is radiative heating of the coldplate from the baseplate (roughly room temp). In the model, the coefficient c is the fit parameter.

P_{testmass} = Fe(is, tm) A_{testmass} \sigma (T_{innershield}^4 - T_{testmass}^4),

where \frac{1}{F_e(is, tm)} = \frac{1}{e_{is}} + (\frac{1}{e_{tm}} - 1)\frac{A_{tm}}{A_{is}} and e_is and e_tm are the emissivities of the inner shield and test mass, respectively. This equation considers radiative cooling of the test mass from the surrounding inner shield. Here, the fit parameter is e_tm. 

Attachment 1 (top plot) shows the results of the fitting. For conductive cooling of the coldplate, the best fit parameter is c=0.62. This means that 62% of the calculated conductive cooling power is actually being delivered to cool the coldplate, according to this model. Another way to look at it is that the constant factors (A, l of copper braid) that are used in the model need a correction of 0.62. Regardless, the model predicts a plateau temperature a few degrees cooler than the data shows. This means there must be a heat source we are not considering that delivers extra heating power at lower temperatures. 

The testmass cooldown best fit parameter is e_tm = 1. I supplied bounds on e_tm from 0 to 1, since it is an emissivity value; the fit hits the upper limit. This is consistent with Koji's result that the calculated test mass emissivity is over 1. It is not clear why/how the test mass is cooled so quickly, since the black paint realistically has an emissivity between 0.5-1. Just like for the coldplate, the current model predicts a plateau temperature lower than what the data shows.

The bottom plot of Attachment 1 shows the difference between the fits and the data. The coldplate model does fairly well at high temperatures, but starts to break down around 100K. Then, other effects must be kicking in that we are failing to consider. 

Next I plan to simplify further and model cooling power as a polynomial of T, and fit for its coefficients. Hopefully this can give insight into the temperature dependence of cooldown curve. 

  2635   Thu Aug 5 09:20:44 2021 AidanLaser2um PhotodiodesOptical design for 2um PD in new cryo chamber

I've sketched out a way to change the beam size on the in-vacuum PD. I think the beam diameter coming from the collimator is 1.2mm, but I need to check this. If we add a telescope outside the vacuum system and put the second lens of this on a translation stage, then this provides us with wide control of the beam size on the PD inside the vacuum system (about 400mm away).

 

 

 

  2634   Wed Aug 4 18:55:58 2021 aaronDailyProgressCryo vacuum chamberloading cantilevers into megastat

This afternoon I met with Aidan and Stephen about near-term plans for the megastat. Aidan and I got familiar with the various viewports, and identified that if we want to set up another window for laser access we would need to move the existing window to the viewport 60 deg clockwise from its current location (at the SE corner of the chamber). We also noted that there is a single instrument RTD currently available (plus three others monitoring each heat shield and the cold head), so setting up two separate measurements each requiring temperature readout simultaneously would require opening up the electrical feedthrough and wiring up another RTD.

This week, I will be installing a clamped cantilever into the existing op lev setup in the cryostat. We will then pumpdown the chamber on Friday, and cool down over the weekend. At the beginning of next week, I will make some Q measurements of the clamped cantilever around 123K, then warm back up so Aidan can set up PD testing at the end of next week or early the following. 

Today, I pulled a moderately smooth cantilever from cryo, and brough it over to QIL to clamp it. I hadn't used this clamp before, and found that the cantilevers Zach was producing in 2018 are larger than the slot in the clamp that was in the megastat. Since the clamping screws are not centered around the cantilever itself, one end of the clamp is touching steel on steel and the other is slightly open. I found in the elog that Zach was using a spare, broken off cantilever piece to balance the clamp. Later, he updated the clamp design and used an alignment jig to set the cantilever in the clamp. I will bring these items from cryo lab and install them in the megastat tomorrow. 

Attachments:

  1. clamp before any changes
  2. View of the indium foil below the clamp
  3. Two cantilevers from cryo, I used the one on the left
  4. The uneven clamping job. Following my first attempt at clamping, I opened the clamp fully and noticed (and removed) Si particulate on the clamping surfaces. This uneven clamp is damaging the cantilever, and/or the cantilever's edges are shedding.
  5. Showing that the clamped cantilever is somewhat too high for the megastat window. The cantilevers Zach was using with this clamp were shorter, and we do have some remaining in the cryo lab. 
  6. Overview of the megastat before covering with foil

Additional photos are on the ligo.wbridge google drive, under Google Photos -> CantileverQ.

  2633   Tue Aug 3 23:56:00 2021 KojiDailyProgressCryo vacuum chamberWarmup started 02 August

- Confirmed the heating stopped in the evening -> The heater was deactivated @~23:00

- Made some measurements and checks - the oplev spot was approximately on the center of the QPD before warming up. Now it is ~4mm above the center (note that the QPD size is 0.5" in dia) (Attachment 2). This corresponds to ~2mrad misalignment.

- Dismantled the OSEM electronics and power supply from the table. The electronics were salvaged into the OMC lab -> to be returned to the 40m.

- A 2" Al mirror package was brought to the OPLEV periscope so that the gold mirror (too thin) can be replaced. (Attachment 1)

  2632   Mon Aug 2 21:51:37 2021 KojiDailyProgressCDSConnecting CTC100 to EPICS/rtcds system

The legit way to restart st.cmd is

systemctl restart CTC100
  2631   Mon Aug 2 17:24:20 2021 RadhikaDailyProgressCDSConnecting CTC100 to EPICS/rtcds system

I added an EPICS channel for the heater power controlled by the Megastat CTC100.

1. Added a function to the protocol file to query the heater power: /opt/rtcds/caltech/c4/target/qil-nfs/CTC100/iocBoot/iocCTC100/protocols/ctc100.proto

2. Created a new channel C4:CTC-MS_HEATER_POWER_VAL in the database file: /opt/rtcds/caltech/c4/target/qil-nfs/CTC100/db/ctc100.db

3. Restarted st.cmd:

cd opt/rtcds/caltech/c4/target/qil-nfs/CTC100/iocBoot/iocCTC100/
./IOC_start_cmd.sh

At this point I confirmed I could access the channel via

caget C4:CTC-MS_HEATER_POWER_VAL

4. Restarted daqd@standiop.service

ssh fb4
sudo systemctl restart daqd@standiop.service
  2630   Mon Aug 2 13:25:32 2021 StephenDailyProgressCryo vacuum chamberWarmup started 02 August

With Test Mass RTD at 119K, and with all of Koji's trials completed, I started the warmup this afternoon.

 - Cryocooler off at 12:41

 - Heater on at 13:05 (forgot to complete this task durming my initial visit).

Anticipated warmup duration of ~ 1 day, as improvements to cooldown (higher emissivity test mass, better conduction to inner shield) should also improve the efficiency of our active warming, which took a bit more than 30 hours last time (ref QIL/2615).

  2629   Sun Aug 1 22:22:00 2021 KojiSummaryCryo vacuum chamberCooling update

The test mass temperature indicates 121K@100hr but there seemed a few sensor glitches for the test mass (𝛥=-4.2K) and the inner shield (𝛥=-0.43K).
So the actual test mass temperature could be 125K.

The temp was read to be 119K@114hr (Attachment 1)

There was very little cooling capability left for the test mass (Attachment 2)

The OSEM reading is now stable @12.3V (Attachment 3)

The raw temp data and the minimal plotting code are attached (Attachment 4)

  2628   Fri Jul 30 18:18:21 2021 KojiDailyProgressCDSConnecting CTC100 to EPICS/rtcds system

[Radhika, Koji]

During the process, we corrected the channel labeling for RTD #3/#4. So  for a few first data points, the numbers for the workpiece and the outer shield were swapped.

  2627   Fri Jul 30 17:28:14 2021 RadhikaDailyProgressCDSConnecting CTC100 to EPICS/rtcds system

[Koji, Radhika]

We were able to successfully integrate the Megastat CTC100 temp data into EPICS and Frame builder. Picking up from my last entry, we completed the following steps:

1. Restarted the EPICS st.cmd service - this "connected the wires" from the CTC100 to EPICS and allowed us to be able to read out live-time channel values. Koji created a script file to restart st.cmd:

cd /opt/rtcds/caltech/c4/target/qil-nfs/CTC100/iocBoot/iocCTC100
./IOC_start_cmd.sh

Note that if these channels need to be edited, this is the script one should call to restart EPICS. At this point, we could get the values by caget commands like

caget C4:CTC-MS_WORKPIECE_TEMP_VAL

P.S. Chris sent us a permanent solution for the service. The process was killed and the service was started by the following command

systemctl restart CTC100

2. Appended new channel names to an existing .ini file (/opt/rtcds/caltech/c4/chans/daq/C0EDCU.ini). This allowed us to record these channels in Frame builder. I was originally going to create a new .ini file with these channels and add the name of the file to master, but we could not find the master file. Plus, instructions of fb4 told us to append to C0EDCU.ini specifically.

3. Restarted daqd@standiop.service on fb4:

sudo systemctl restart daqd@standiop.service

We used DataViewer to verify that the channels were being recorded. Success!

  2626   Fri Jul 30 14:44:56 2021 StephenThings to BuyCryo vacuum chamberUpgrades and updates in advance of PD testing

(Aidan, Stephen, Koji)

Building off of QIL/2597 after more thorough discussion in Mariner meeting today. Aidan and I will confirm details today and make moves toward installation of PDs next week.

Necessary capabilities (note: no need to scavange anything from the IRLabs dewar):

 - Cold temperatures = ready (via conductive mounting we have seen workpiece ~ 80 K, workpiece heating and CTC100 temp control is demonstrated)

 - Optical interface = ready (existing 1700 nm AR-coated window will be used at 2 micron, input power will just be calibrated with a power meter)

 - Electrical interface = almost ready, pending cabling (the cryo vacuum chamber has RTDs instrumented, so we just need the leads for the PDs, and we can create Cu twisted pair leads with in-vac crimp/solder sockets a la Koji's OSEM cabling) (also need in-air cabling with DB9 plug - trivial)

Improvements in advance of PD testing:

 - RTD cabling and Heater cabling (in vacuum) should be split with in-vac pins and insulated with PTFE tube - Koji has the magic material recommendations

Desired improvements (not necessarily in advance of PD testing):

 - Cu solid linkage (being fabricated).

 - Inner radiation shield should be clamped well to cold plate (consistent with most recent trial, but do we want better/more clamps?).

 - RTD mounting option on shields without cryo varnish (new threaded hole, new clamps).

 - RTDs consistent with planned Mariner RTDs (ref. QIL/2590).

 - Heater mounting should be directly to the workpiece via an improved clamp on the 2" x 2" grid (rather than on unused Si cantilever workpiece holder).

  2625   Fri Jul 30 12:22:56 2021 KojiSummaryCryo vacuum chamberCooling curve comparisons

In all aspects, the latest cooling shows the best performance thanks to better thermal connection, thermal isolation, and the black paint.

- The cold head cooling is faster and cooler

- The inner shield cooling is faster

- The test mass cooling is faster

  2624   Fri Jul 30 12:22:15 2021 RadhikaDailyProgressCDSConnecting CTC100 to EPICS/rtcds system

Currently the CTC100 temperature data for Megastat is extracted via ethernet (telnet) through a python file. The file queries the device for temperature readings every minute and stores the data to a .txt file on QIL-WS1. Our goal is to connect the CTC100 data directly to SLOW EPICS in the QIL.

It has been helpful that the other CTC100 in the QIL (henceforth called the original CTC100), which is used for temp monitoring of the small PD testing chamber, had already been integrated into EPICS. I located the relevant files (from QIL-WS2) under /opt/rtcds/caltech/c4/target/qil-nfs/CTC100/. This will now be the called parent_directory.

The CTC100 protocol was already defined at parent_directory/iocBoot/iocCTC100/protocols/ctc100.proto. I added protocol functions corresponding to the commands I would need for querying the Megastat CTC100, of the form:

read_MS_WorkPiece {
    out "WorkPiece?";
    in "%f";
    @init {
      out "WorkPiece?";
      in "%f";
    }
}

I created a function block for each of the 4 channels read by the Megastat CTC100.

Next, I located the st.cmd file: parent_directory/iocBoot/iocCTC100/st.cmd. I added the following line to configure the port to the new CTC100, copying the sytax of the original CTC100:

drvAsynSerialPortConfigure("CTCMS", "10.0.1.158:23", 0, 0, 0)

The .db file for channels corresponding to the original CTC100 is found at parent directory/db/ctc100.db. I added blocks for the new EPICS channels to write the CTC100 data into:

record(ai, C4:CTC-MS_WORKPIECE_TEMP_VAL) {
    """
    field (INP, "@ctc100.proto read_MS_WorkPiece CTCMS")
    """
}

Here, the input field indicates the path to the protocol and which function in the protocol to call; and which port to communicate with. I added a block for each of the 4 channels of the Megastat CTC100.

The next step should be to restart the EPICS service so that these channels can be created. I have not been able to locate the right service file to restart, but hopefully once I do, I should be able to call caget on one of the channels and see a real-time value.

Next, I will create a .ini file to load into the frame builder service, so that the frame builder can record the new channels into frames and save records of data. I tried to look for this .service file with the help of Aidan and Anchal, but we have not yet been able to locate it. I hope to solicit Chris' help for both this task and the one above.

 

  2623   Fri Jul 30 09:48:11 2021 RadhikaDailyProgressCryo vacuum chamberCooling model updates from Koji's analysis

I replicated Koji's recent cooldown analysis on data prior to painting the test mass with black coating. The model first considers conductive cooling of the coldplate + inner shield from the cold head, via copper braid. Then it considers radiative cooling of the test mass from the coldplate + inner shield. 

To model the conductive cooling of the coldplate + inner shield, I used:

dT_coldplate/dt = C * k_Cu(T) * A_Cu/l_Cu * (T_coldhead - T_coldplate) / (Cp_Al(T) * m_coldplate)

where A_Cu and l_Cu are the cross-sectional area and length of the copper braid. I used a temperature-varying heat capacity of Cu and specific heat of Al. In order to align this model with the data, I found that the constant C=0.085. I am not sure what extra factors should be contributing to this scaling, but once it is added, the model aligns well with the two time constants apparent in the data [Attachment 1]. I will connect with Koji to determine what he considered here / if there is something I am missing.

I then took the aligned coldplate + inner shield cooling model to consider the radiative cooling of the test mass. I used:

dT_tm/dt = Fe * sigma * A_tm * (T_coldplate^4 - T_tm^4) / (Cp_Si * m_tm)

where we assume T_coldplate is the temperature of the coldplate + inner shield. Fe is the emissivity coefficient Koji considers in his analysis, which I found to be consistent with his result: 0.15. As he stated in a previous entry [2617], Fe can be broken down as:

1/Fe = 1/e_tm + (1/e_surr - 1)*A_tm/A_surr,

where e_surr and A_surr are the emissivity and area, respectively, of the surrounding coldplate and inner shield. Using e_surr=0.07 (rough Al), we get that an Fe value of 0.15 corresponds to a test mass emissivity of 0.18. This is slightly lower than Koji's value, due to differences in our calculated surface areas, but otherwise consistent.

A key point is that once the conductive cooling of the coldplate is modeled accurately (with a fudge factor of 0.085), the radiative cooling model of the test mass lines up well with the data without the need for another fudge factor. Note that the radiative cooling model above does not use a temperature-varying specific heat of Si [Attachment 1]. If a temperature-dependent value is used, we end up with the test mass cooldown model seen in Attachment 2. This causes the model to diverge from the data, so another factor might be missing in the model. Perhaps using temperature-dependent emissivities will correct for the deviation and cause even better agreement. This is a future step for the model.

Lastly, the painting of the test mass will increase its emissivity value, strengthening the radiative link between the test mass and its surroundings. (Koji has already posted updates on this cooling trend, and I will use this data once I obtain a copy.) Based on Koji's entry [2617], we can consider a new e_paint of 0.5 and 1. Attachment 3 compares radiative cooling models of the test mass using different emissivity values. We can expect that if the coating performs as expected, the test mass can reach 123K between ~87-110 hours. A next step is to plot the cooldown data for the painted test mass to see how accurate this prediction is. 

I will next aim to understand the 0.085 fudge factor needed to align the conductive cooling model with the coldplate cooling data. I will also add a fitting feature to directly spit out the optimal factors needed in both conductive and radiative cooling. 

 

  2622   Thu Jul 29 13:11:17 2021 KojiSummaryCryo vacuum chamberCooling progress: Update

The current cooling curve suggests that the radiative cooling factor Fe (black body =1) increased from 0.15 to 0.5.

Update: The test mass temp is reaching 200K at ~27hrs. cf previously it took 50hrs
Update: The test mass temp is 170K at ~41.5hrs.


OSEM illumination & photodetector efficiency has been kept increasing @41.5hrs

  2621   Thu Jul 29 00:42:38 2021 KojiSummaryCryo vacuum chamberThe test mass successfully suspended

[Stephen Koji]

Road to cooling down

  • The suspension with the test mass was installed in the chamber again
  • Looking at the oplev beam, we jiggled the wire loop position to adjust the alignment approximately.
  • The oplev beam was aligned more precisely.
     
  • We intentionally kept the OSEM at the "fully-open" position, while it is still close to the magnet so that we can have some actuation.
  • The coil driver was tested before closing the chamber, but it did not work.
    The coil itself was still intact, and the mirror was responding to the coil current if the coil current of ~100mA was applied from a bench power supply with the current ~100mA).
    So the problem was determined to be external.
     
  • Once we were satisfied with the oplev/OSEM conditions, the inner and outer lids were closed. Then the chamber was closed.
     
  •  Started pump down.
  • Started cooling down @18:30 / started temp logging too. Log filename: temp_log_cool_down_20210728_1830.txt

The photos were uploaded to Google Photo of WB labs.


The coil driver issue was resolved:

  • It was necessary to take care of the enable switch. Made a DB9 short plug for this purpose.
  • The output R was 1.2K (i.e. 2.4K across the + and - outputs). We needed ~10x more to see visible motion of the mass
  • e.g. The internal gain of the driver is x1.1. If we connect 5VDC input across the diff input of the driver yields, +11V shows up across the outputs of the final stage.
    If the R across the coil is ~100Ohm, we get ~100mA.
  • Soldered 6 x  330Ohm (1/8W) in parallel to 1.2K R_out. -> This ended up 51.5Ohm x2 across the coil. Each R=330 consumes ~1/10W. ->OK

Checking the DAQ setup / damping loop

  • DAQ setup
    • ADC: QPD X->FM16 / Y->FM17 / S->FM18 / OSEM-> FM19
    • DAC: CH11 -> Coil Driver In
  • Connected FM16 and FM17 to the coil drive by setting C4:TST-cdsMuxMatrix_12_17 and C4:TST-cdsMuxMatrix_12_18 to be 1.0
  • It was not obvious if the coil could damp the rigid body modes.
    • Actating the magnet caused Yaw motion most. Some Pitch motion too.
    • Configured FM16 and FM17 for the damping loop.
      • Filter Bank #1: [Diff0.1-10]  Zero 0.1Hz / Pole 10Hz
      • Filter Bank #10: [Anti Dewht]  Zero 1&200Hz / Pole 10&20Hz
    • Tried various damping gain. The mass was moving too much and the proper gain for the damping was not obvious.
    • So, the initial damping was obtained by shorting the coil at the coil in of the sat amp unit. (Induced current damping)
    • Once the test mas got quieter, it was found that -0.01 for FM16 could damp the yaw mode. Also it was found that +0.1 for FM17 could damp the pitch mode. (But not at once as the filters were not set properly)
       
  • TF measurement for calibration
    • The beam was aligned to the QPD
    • The test mass was damped by using the damping loops alternately 
    • Taken a swept sine measurement Filename: OSEM_TF_210729_0243.xml
      Recorded the time, saved the data, and took a screenshot
      • This measurement was taken @T_IS=252K / T_TM=268K @t=8hr (2:30AM), Rcoil=15.6Ohm
    • Second measurement Filename: OSEM_TF_210729_2147.xml
      • @T_IS=172K / T_TM = 201K @t=27.5hr (10PM), Rcoil=10Ohm
    • 3rd measurement Filename: OSEM_TF_210730_1733.xml
      • @T_IS=116K / T_TM = 161K @t=47hr (5:30PM), Rcoil=?
    • 4th measurement Filename: OSEM_TF_210731_2052.xml
      • @T_IS=72K / T_TM = 134K @t=75hr (9:30PM), Rcoil=6.0Ohm

OSEM LED/PD

  • The Satellite amp brought from the 40m is used as-is.
  • The initial OSEM reading was 8.8V, this corresponds to ~30000cnt.
  • As the OSEM was cooled, this number was increasing. To avoid the saturation, a voltage divider made of 4x 15kOhm was attached. I didn't expect to have the input impedance of the AA filter (10K each for the diff inputs), this voltage divider actually made 18.24V across POS and NEG output to be 5.212V to the AA fiter. So the voltage division gain is not 0.5 but 0.2859.
  • This made the ADC range saved, but we still have a risk of saturating the PD out. If this happens. The PD TIA gain will be reduced before warming up.
    -> The TIA and whitening stages use AD822, and the diff output stage uses AD8672. AD822 can drive almost close to rail-to-rail. AD8672 can drive upto ~+/-14V.

There was not enough time for the QPD calib -> Tomorrow

  2620   Wed Jul 28 00:59:47 2021 KojiSummaryCryo vacuum chamberThe test mass successfully suspended

[Stephen Koji]

While Stephen worked on the RTD reattachment, I worked on the suspension part.

- First of all, we found that the magnet was delaminated from the silicon mass (Attachment 1). It was bonded on the test mass again.

- The suspension frame was tweaked so that we have ~max suspension length allowed.

- The first attempt of suspending the mass with steel wires (0.0017" = 43um dia.) failed. Stephen and I went to downs and brought some reels.

- I chose the wire with a diameter of 0.0047" (= 119um) (Attachment 2). ~8x stronger! The suspension was successfully built and the mass is nicely sitting on the 4 strain releasing bars (improvised effort). (Attachments 3/4)

We can install the suspension in the chamber tomorrow (today, Wed)!

 

  2619   Mon Jul 26 22:49:00 2021 KojiSummaryCryo vacuum chamberAquadag painting

[Stephen Koji]

We decided to paint the silicon test mass with Aquadag to increase the emissivity of the test mass.

Stephen brought the Aquadag kit from Downs (ref. C2100169) (Attachment 1)

It's a black emulsion with viscosity like peanut butter. It is messy and smells like squid (Ammonium I think) (Attachment 2)

We first tried a scoop of Aquadag + 10 scoops of water. But this was too thin and was repelled easily by a Si wafer.
So we tried a thicker solution: a scoop of Aquadag + 4 scoops of water. (Attachment 3)

The thicker solution nicely stayed on the Si wafer (Attachment 4)

We want to leave the central area of the barrel unpainted so that we can put the suspension wire there without producing carbon powder. (Attachment 5)
1.5" from the edge were going to be painted. The central1" were masked.

The picture shows how the Si test mass was painted. The test mass was on a V-shaped part brought from the OMC lab. The faces were also painted leaving the mirror, while the place for RTD, and the magnet were not painted. (Attachment 6)

It looked messy while the painting was going, but once it started to dry, the coating looks smooth. It's not completely black, but graphite gray. (Attachment 7)

After the test mass got dry, another layer was added. (Attachment 8)

Then made it completely dry. Now the mask was removed. Nice! (Attachments 9/10)

  2618   Mon Jul 26 01:30:42 2021 KojiSummaryCryo vacuum chamberPrep for the 2nd cooling of the suspension

Updated Jul 26, 2022 - 22:00

 

  1. Reconstruct the cryostat
    1. [Done] Reinstall the cryo shields and the table (Better conductivity between the inner shield and the table)
    2. [Done] Reattach the RTDs (Inner Shield, Outer Shield)
      -> It'd be nice to have intermediate connectors (how about MIllMax spring loaded connectors? https://www.mill-max.com/)
    3. Reattach the RTD for the test mass
  2. Test mass & Suspension
    1. [Done] Test mass Aquadag painting (How messy is it? Is removal easy? All the surface? [QIL ELOG 2619]
    2. [Done] Suspension geometry change (Higher clamping point / narrower loop distance / narrower top wire clamp distance -> Lower Pend/Yaw/Pitch resonant freq)
    3. [Done] Setting up the suspension wires [QIL ELOG 2620]
    4. [Done] Suspend the mass
  3. Electronics (KA)
    1. [Done] Coil Driver / Sat Amp (Power Cable / Signal Cables)
    2. Circuit TF / Current Mon
    3. [Done] DAC wiring
    4. [Done] Damping loop
  4. Sensors & Calibration (KA)
    1. [Done] Check OSEM function
    2. [Done] Check Oplev again
    3. Check Oplev calibration
    4. [Done] Check Coil calibration
    5. Use of lens to increase the oplev range
    6. Recalibrate the oplev
  5. DAQ setup (KA)
    1. [Done] For continuous monitoring of OSEM/OPLEV
  2617   Sun Jul 25 21:45:46 2021 KojiSummaryCryo vacuum chamberAbout the radiation heat transfer model

The following radiation cooling model well explained the cooling curve of the test mass (until ~150K)

\dot{Q}=0.15 A\,\sigma (T_{\rm SH}^4-T_{\rm TM}^4)

where dQ/dt is the heat removed from the test mass, A is the surface area of the test mass, \sigma is the Stefan-Boltzmann constant, T_SH and T_TM are the temperatures of the surrounding shield and the test mass.

Can we extract any information from this "0.15"?


I borrowed "Cryogenic Heat Transfer (2nd Ed)" by Randall F. Barron and Gregory F. Nellis (2016) from the library.
P.442 Section 8.5 Radiant Exchange between Two Gray Surfaces can be expressed by Eq 8.44

\dot{Q} = F_e F_{1,2} \sigma A_1 (T_2^4-T_1^4)

where T_i is the temperature of objects 1 and 2. For us, OBJ1 is the test mass and OBJ2 is the shield. A1 is the surface area of A1. F_1,2 is the view factor and is unity if all the heat from the OBJ1 hits OBJ2. (It is the case for us.)

F_e is an emissivity factor.

The book explains some simple cases in P 443:

Case (a): If OBJ2 is much larger than OBJ1, F_e = e_1 where the e_i is the emissivity of OBJi. This means that the radiated heat from OBJ1 is absorbed or reflected by OBJ2. But this reflected heat does not come back to OBJ1. Therefore the radiative heat transfer does not depend on the emissivity of OBJ2.

Case (b): If OBJ1 and OBJ2 has the same area, \frac{1}{F_e} = \frac{1}{e_1} + \frac{1}{e_2} -1. The situation is symmetric and the emissivity factor is influenced by the worse emissivity between e1 and e2. (Understandable)

Case (c): For general surface are ratio,  \frac{1}{F_e} = \frac{1}{e_1} + \left(\frac{A_1}{A_2}\right)\left(\frac{1}{e_2} -1 \right ). OBJ2 receives the heat from OBJ1 and reradiates it. But only a part of the heat comes back to OBJ1. So the effect of e2 is diluted.

For our case, OBJ1 is the Si mass with DxH = 4in x 4in, while the shield is DxH = 444mm x 192mm. A1/A2 = 0.12.
We can solve this formula to be Fe=0.15. e1 = (0.147 e1)/(e2-0.0178).

Our inner shield has a matte aluminum surface and is expected to have an emissivity of ~0.07. This yields the emissivity of the Si test mass to be e1~0.2

How about the sensitivity of e1 on e2? d(e1)/ d(e2) = -0.95 (@e2=0.07).


Can Aquadag increase the radiative heat transfer?

Depending on the source, the emissivity of Aquadag varies from 0.5 to 1.
e.g. https://www.infrared-thermography.com/material-1.htm / https://www.mdpi.com/1996-1944/12/5/696/htm

  • Assuming Aquadag's emissivity is ~1
    • If only the test mass is painted, F_e increases from 0.15 to 0.39 (x2.6)
    • If the inner shield is also painted, F_e increases to 1, of course. (pure black body heat transfer)
    • If shield panels are placed near the test mass with the inner surface painted, again F_e is 1.
  • Assuming Aquadag's emissivity is ~0.5
    • If only the test mass is painted, F_e increases from 0.15 to 0.278
    • If the inner shield is also painted, F_e increases to 0.47.
    • If shield panels are placed near the test mass with the inner surface painted, F_e is 0.33 assuming the area ratio between the test mass and the shield panels to be unity.

It seems that painting Aquadag to the test mass is a fast, cheap, and good try.

  2616   Fri Jul 23 20:53:40 2021 KojiSummaryGeneralJul 17, 2021: Canon camera / small silver tripod / macro zoom lens / LED ring light returned / ELectronics borrowed

[Returned] Brought one HAM-A coil driver (D1100687 / S2100619) and one Satellite Amplifier (D1002818 / S2100741) from the 40m

Also brought some power cables.

Brought ~1m of 0.0017" (~43um) misical wire. This will make the tension stress be 341MPa. The safety factor will be ~7.

 

  2615   Thu Jul 22 22:03:45 2021 KojiSummaryCryo vacuum chamberTest mass heating in progress (2021/07/21 ~ 2021/07/23)

- Temperature Log updated 2021/7/23 12:00 Heating Ended

- Assuming reaching the room temp at ~30hrs and heating power saturated at 22W: Predicted heat injection 30*3600*22 = ~2.4MJ

Update from Stephen
- Note that we can check logging accuracy against the snapshot (timestamp 20210723_1113).
If my math is correct, this would be time = 37.35 38.35 hours

Update from KA
=> The corresponding time in sec is 138060 sec
The raw data line for the corresponding time is:

138016.839614, 295.805, 306.678, 302.518, 312.401, 0.000, 0.000, -0.001, 0.621, 0.622, 1.429, 0, 0, NaN, NaN, NaN
The values on the photo 295.806, 306.677, 302.518, 312.401 ==> Well matched. Victory!

  2614   Wed Jul 21 21:05:59 2021 KojiSummaryCryo vacuum chamberTest mass cooling (2021/07/16 ~ 2021/07/21)

[Stephen and Koji for discussion / Koji for the execution]

1. Temperature Trend

See [QIL ELOG 2611] for the updated temp log and the cooling model.

Considerations for the next cycle:
-> How can we accelerate the cooling? It seems that the table cooling is conduction limited. Improve the cold head connection.
-> We want to move the RDTs
-> How can we improve radiative cooling?

2. Oplev Trend (Attachment 1)

Sum: The beam has been always on the QPD (good). See also Attachment 2

X&Y: In the first few hours the beam drifted in -X and then +X while Y had slow continuous drift in +Y. ~11hours later sudden drift in -Y and totally saturated. Also -X saturation observed @~16hrs. Again +Y drift was seen @~25hrs. The totally saturated in -X and +Y.
They may be related to the drift of various components with various cooling time scale.

Visual check: ~2mm shift in X&Y is visually observed. Attachment 2

-> How can we quantify the drift? What information do we want to extract?

3. OSEM and the magnet

The magnet is intact. And the suspension seemed still free after cooling (Attachment 3)
Significant misalignment was not visible. No visible damage by cooling was found. The coil is alive and the PD/LED are also intact. Fluke showed that they are still diodes, but their function was not checked.

The coil resistance changed from 16Ohm -> 4.2Ohm. For the 16Ohm, 2 Ohm was from the wire. Let's assume we still have 2Ohm overhead -> The coil R changed from 14->2.2. This corresponds to the coil temperature of the order of ~100K. This is not so crazy.

Some actuation current was applied to the magnet. For this test, the oplev was realigned.
First, some ~300mA current pulses were applied to the coil. The ringdown of the yaw mode was visible. Then the DC current of 100mA was applied. This didn't make visible change on the spot position but the data showed that there was a DC shift.

-> We prefer to have a softer suspension for the next test.

4. CTC100 logging

During the cooling we kept having inaccurate data logged compared with the displayed data on the screen of CTC100.
As soon as the cooling logging was stopped, telneting to CTC100 was available. So, I telnetted to the device and sent the data transfer command ("getOutput"). Surprisingly, the returned values agreed with the displayed values.
So my hypothesis is that somehow the data strings are buffered somewhere and gradually the returned values get delayed. From the behavior of the device, I imagined that the fresh telnet connection gives us the latest data and there is no buffering issue.

So I tweaked the data logging code to establish the telnet connection every time the values are asked. The connection is closed after the every data acquisition. I like this as we can also make the test connection between each data acquisition points, although I have not tried it yet. The code is in the same folder named ctc100_controller_v2.py

5. Heating

Now I thought that I did all I wanted to do this evening, so the heater was turned on at ~20:50, Jul 21. The heating power saturated at 22W, which is the set limit.

  2613   Wed Jul 21 14:53:28 2021 KojiSummaryGeneralJul 17, 2021: Canon camera / small silver tripod / macro zoom lens / LED ring light borrowed -> QIL

See https://nodus.ligo.caltech.edu:8081/40m/16250

  2612   Wed Jul 21 13:14:11 2021 PacoLab Infrastructure2micronLasersBrimrose AOM and amplifier

Yesterday I came in the QIL and performed an express kidnapping of the 2um in fiber AOM (Brimrose) and the 5 W RF amplifier that was hooked to the RF in port (though it seems it saturates at ~ 600 mW from past elogs). I will test it with the 1419 nm ECDL fiber pickoff port to see that it works and if it doesn't I will reinstall it in the 2um testing facility.

  2611   Tue Jul 20 17:28:30 2021 KojiSummaryCryo vacuum chamberA cooling model (Temp Log 210716_2255)

Updated the model the latest log data with cooling prediction

  • The radiative cooling is expected to be the dominant cooling mode.
  • It will take ~3 more days to reach 123K. We don't need to wait for it.
  • For more informative temp data, we need the temperature of the inner shield and the table.

  • We know the cold head temp from the measurement. For the prediction, the constant cold head temp of 65K was assumed.
  • The table temp was estimated using conductive cooling model + linear empirical dependence of the conductivity on the temp
  • The constant specific heat of the silicon mass (0.71 J/K/g) was assumed. This may need to be updated.
  • The radiative cooling is given from Stefan–Boltzmann law with the emissivity of 0.15 for both the shield and the mass.
     
  • The conductive cooling of the test mass was estimated using: Wire diameter 0.017" (=0.43mm), 4 wires, length of ~10cm (guess), no thermal resistance at the clamps (-> upper limit of the conductive cooling)

Radiative cooling already gives us a good agreement with the measured temp evolution for the test mass. The conductive cooling is not significant and does not change the prediction.


Updated the plot with the new data (2021/7/21 12:30PM)

  2610   Tue Jul 20 11:33:52 2021 KojiSummaryCryo vacuum chamberA cooling model (Temp Log 210716_2255)

A naive cooling model was applied to the cooling curve.
A wild guess:

- The table temp is the same as the test piece temp as measured on 2021/7/9
- The inner shield temp is well represented by the table temp
- The specific heat of Si is almost constant (0.71 [J/(g K)] between 300K~200K

Radiative cooling:
The curve was hand-fitted by changing the emissivity of the inner shield and the silicon mass. I ended up having the same values for these to be 0.15.
Surprisingly well fitted!

Conductive cooling:
The conductive cooling through the wire does not fit the cooling curve, although the quantitative evaluation of the wire conductivity needs to be checked carefully.

Appendix:
Stephen shared attachments 2 and 3, which contain insights on the wire used to hang the Si mass. .017" diameter Music Wire from California Fine Wire, 2004 vintage, borrowed from Downs High Bay.

  2609   Mon Jul 19 17:21:19 2021 KojiSummaryCryo vacuum chamberTemp Log 210716_2255

Temp Log on Jul 19 2021 17:20

I wonder what is the heat transfer mode for the test mass right now. Radiative? or Conductive through the wires?

 

  2608   Mon Jul 19 15:57:17 2021 StephenSummaryCryo vacuum chamberTemp Log 210716_2255

Uh oh, review of the cooldown plot from the previous cooldown (QIL/2603) shows workpiece temperature of ~92 K at conclusion, while a temperature of 65K was observed in the CTC100 readout (Attachment). The logging of the warmup is consistent with the CTC100 image, as the logging started a few minutes after the warmup was started, and the warmup "5 minutes after starting" temperature of ~ 71 K is a practical temperature.

Seems to be something weird going on here, we will need to have Radhika take a look on her return (and continue taking photos of the CTC100 whenever we stop by).

Quote:

Temperature log for the first 2 hours (Attachment 1)

I wonder why the temperatures displayed on CTC100 and the ones logged are different...?

 

 

  2606   Sat Jul 17 00:55:41 2021 KojiSummaryCryo vacuum chamberTemp Log 210716_2255

Temperature log for the first 2 hours (Attachment 1)

I wonder why the temperatures displayed on CTC100 and the ones logged are different...?

 

  2605   Fri Jul 16 23:28:24 2021 KojiSummaryCryo vacuum chamberSus Test Work 07/16/2021

[Stephen Koji]

We started cooling down of the test mass.

Venting

- Stephen vented the chamber at 2PM. An optical port was moved to see the OSEM from the back.

OSEM wiring

- Brought DSub crimp sockets from the 40m. We picked up 3x 1m LakeShore WCT-RB-34-50 (twisted silver-plated copper, 34 AWG with Teflon insulation). The ends of the wires were dangled so that crimping is possible. A single wire resistance was measured to be ~1Ohm at room temp. (Attachment 1)

- OSEM pin out / backside view (cable going down) (Attachment 2)

|   o   o   o |
| o   o   o   |                 Wire
  ^ ^ ^ ^ ^ ^---PD K        ---- R3
  | | | | |-----PD A        ---- B3
  | | | |-------LED A       ---- B2
  | | |---------LED K       ---- R2
  | |-----------Coil End    ---- B1
  |-------------Coil Start  ---- R1


Twisted Pair 1: (R1&B1) with 1 knot  at the feedthru side
Twisted Pair 2: (R2&B2) with 1 knot  at the feedthru side
Twisted Pair 3: (R3&B3) with 1 knot  at the feedthru side

Dsub feedthru in-air pinout (Mating side)

    1  2  3  4  5
\ o  o  o  o  o /
 \ o  o  o  o  /
   6  7  8  9

Pin1 - Coil Start
Pin6 - Coil End
Pin2 - LED K
Pin7 - LED A
Pin3 - PD A
Pin8 - PD K

Pin1-6 R=16Ohm
Pin2-7 Diode V (with Fluke) 1.18V (Pin2 black probe / Pin7 red probe)
Pin3-8 Diode V (with Fluke) 0.7V (Pin3 red probe / Pin8 black probe)

- OSEM pin out / backside view (cable going down)

Suspension installation (Attachment 3)

- The sus frame was moved into the chamber

- We measured the test mass dimension before installation: L 3.977" D 4.054"

- The attached mirror size is 1"x1" made of SUS #8 (?)

- The mass was suspended. The height / rotation of the mass was adjusted so that the reflecting mirror is visible from the oplev window and also the OSEM magnet is visible from the OSEM window.

- The OSEM was placed on an improvised holder. (Attachment 4)

Oplev installation

- ...Just the usual oplev installation. Adjusted the alignment and the return beam hits right next to the laser aperture. This beam was picked off by a mirror and steered into a QPD. (Attachments 5/6)

- The lever arm length is ~38" (960mm) -- 9" internal / 29" external
- The oplev signal is shaking so much and occupying ~50% of the full scale. Added a lens with f=250 to make the beam bigger, but the improvement was limited.

Pumping down

- Started ~8:30PM?

DAQ setup

- Wired 3 BNC cables from the table to the DAQ rack. CHX/Y/S are connected to ADC16/1718ch.

- The real-time processes seemed dead. Looked at [QIL ELOG 2546] to bring them up. TIM/DAQ error remains, but the data stream seems alive now. Leave it as it is.

Cooling

- Temp Logging started. Filename: temp_log_cool_down_20210716_2255.txt

- Cryocooler turned on. ~10:55PM

- Confirmed the cold head temp was going down. The cold head temp is 75K at 0:30AM

OSEM photo

- An example photo was taken from the rear window. The attempt with 40m's Canon failed. Attachment 7 was taken with KA's personal compact camera with a smartphone LED torch. The gap between magnet and OSEM is highly dependent on the view axis. So this is just a reference for now.

  2604   Thu Jul 15 23:37:53 2021 KojiSummaryCryo vacuum chamberBonding work for the prep of the preliminary suspension test

[Stephen / Koji]

Bonding work for the prep of the preliminary suspension test

- 1" sq mirror-ish polished SUS piece was bonded to a face of the silicon mass. We chose the location right next to a line on the barrel. (Attachment 1)

- The mass was flipped with two more same thickness pieces used for the spacers to keep the mass horizontal.

- A pair of an OSEM and dumbbell-magnet was brought from the 40m (courtesy by Yehonathan). The magnet was glued on the mass at the opposite position of the attached mirror because the optical ports are going to be arranged to share an axis. A piece of cryo varnish was also painted with a piece of cigarette paper at the center of the mass so that we can attach an RTD. (Attachment 2)

Next Things To Do (Attachment 3)

  • Vent the chamber
  • We will move an optical port to the opposite position of the other port.
  • A DB9 feedthru is going to be installed.
     
  • Suspension
    • Move the sus frame in the chamber
    • Suspend the mass
  • Sensor arrangement
    • Set up the oplev
    • Hold the OSEM at the height of the magnet
    • Set up a camera to observe the magnet-OSEM clearance
    • We improvise the DB crimping sockets so that we can electrically connect the OSEM (optional)
  • Pump down / cool down the chamber
    • The main target of the cooling is to check the cooling capability of the test mass mainly with radiative cooling.
    • An optional target is to observe the misalignment as a function of the temperature -
      • -> Oplev signals are to be connected to CDS / check if CDS is logging the data
    • Check if the OSEM/magnets survive the thermal cycle
    • If possible we can try to actuate the OSEM / check the LED/PD function at the cryo temp
       
  2603   Thu Jul 15 23:34:17 2021 KojiSummaryTempCtrlTemprerature Log for cooling down / warming up

[Stephen Koji Radhika]

Stephen and Radhika worked on the cooling down and warming up of the cryostat with the cold head RTD attached using a spring-loaded screw. No other configuration changes compared to QIL/2599. Here are the temperature log plots. Photos of spring clamped RTD are outstanding, but the clamp is the same as the workpiece pictured in QIL/2599/Attachment 12.

  2602   Mon Jul 12 14:42:42 2021 StephenDailyProgressCryo vacuum chamberRTD attached to coldhead with spring clamp, Si mass to be installed this week

Brief summaries of the last week's progress and the coming week's plans (plots will be posted soon!):

- progress Friday 09 July: Opened the cryostat up at the cold head, and attached an RTD to the cold head with a spring clamp (instead of relying purely on the cryo varnish).

- progress Monday 12 July: Found 65 K workpiece temp and 63 K cold head temp. RTD was apparently held successfully by spring clamp, and we will continue to collect cold head temperature in future runs. Warmup was started, with old data collection completed (cooldown_20210709) and new data collection commenced (warmup_2021_07_12). Note that warmup started at 1:14 pm, and it took me ~ 5 minutes to stop and restart the script to changeover to the warmup data collection.

- table plan Wednesday 15 July: Complete in-air optical layout. Make one flat face of Si mass reflective.

- chamber plan Thursday 16 July: Open up main volume and drop in frame with Si mass. Connect RTDs. Start cooldown. Confirm cooldown is going ok (optical alignment, especially), and revert if necessary before things get too cold.

- table plan Friday 16 July: Maybe measure stuff, maybe better to wait till coming week and use controlled heating to hit different temperature setpoints.

 

  2601   Fri Jul 9 13:44:39 2021 RadhikaSummaryCryo vacuum chamber1D cooling model updates

*Takeaway*: The current 1D cooling model is getting closer to matching our observed cooling trends, mainly in the lower temperature limit. The predicted time constant is still much smaller than we are seeing in reality (by about a factor of 3), but this can potentially be improved by revising specific heat values and/or dimensional estimates for chamber components.

The model uses the known cooling power of the cold head [attachment 2] and considers radiative heat from the outer shield, baseplate (bottom lid), and mylar wrapping around braid. I increased the complexity of the script by solving a system of ODEs (for braid and coldplate temperature) simultaneously instead of assuming the temperatures are equal at all times, and solving only 1 ODE. This resulted in the model's lower temperature limit prediction matching our observed data, at ~66 K. 

The model still predicts a much smaller time constant than we are seeing. This is affected by specific heat values for Cu and Al, along with dimensional estimates of the coldplate and braid (AKA how much mass is being cooled). It is possible that these values are being underestimated in the model, which would lead to the smaller time constant. Currently the model uses constant values for the specific heat of Cu and Al (room temperature). But since specific heat increases with temperature, accounting for temperature dependence would lower the specific heat values and shift the model in the opposite direction (towards an even smaller time constant). Therefore I suspect the model is underestimating the mass of the coldplate, though I am unsure if this would completely correct the discrepancy. 

If the term (specific_heat * density * volume) of the coldplate (Al) is increased by a factor of 4, the model resembles the data well [attachment 3]. 

  2600   Fri Jul 9 10:57:58 2021 RadhikaSummaryCryo vacuum chamberCTC100 temperature extraction

I wrote a python script to extract temperature data from the CTC100 via ethernet, for monitoring cooldown/warmup of Megastat. This is intended to replace USB data extraction, which requires the user to manually insert/remove the stick and plug into a computer.

The script queries the CTC100 every ~60 seconds for the latest temperature values (the frequency can be supplied as a parameter, but default is 60s). The script writes line-by-line to a .txt file and also plot the outputted data once collection is terminated.

Here is a gitlab link to the script: https://git.ligo.org/voyager/mariner40/-/blob/master/CryoEngineering/ctc100_controller.py. It is also found on the QIL workstation at /home/controls/CTC100/ctc100_controller.py. To run from the workstation, open terminal to /home/controls (home). Then:

cd CTC100
python ctc100_controller.py --filename='tutorial'

 Here, 'tutorial' stands in for the desired filename for the outputted data. The script will start pulling data and will print each line to the terminal. It will continue printing and logging the temperature values until the user hits Ctrl+C in the terminal. This will terminate the script and output the final data file. The file is saved as a .txt file in /home/controls/CTC100/data.

  2599   Tue Jul 6 18:07:20 2021 RadhikaDailyProgressCryo vacuum chamberCooldown 7/1-7/6

I've attached cooldown data from 7/1-7/4, which was extracted via ethernet from the CTC100. Initially I was having issues getting the curves smooth; the data seemed very choppy and I assumed it was a device or ethernet issue. Turns out the csv file outputted by my script would cast all floats to integers if I opened it and saved, which was very strange. I'm still not sure why this happens, but my workaround is to not edit the csv at all after it is outputted.

The workpiece temperature stabilized at ~65.8 K, just below 66 K (last cooldown). This makes sense given the few minor tweaks we made in between (removed shorting Al foil, adjusted mylar / peek sheet insulation). The time constant is also consistent (~36.4 hrs). 

Unfortunately the RTD on the cold head appears to have detached yet again. It seems to have happened around the same time as the last cooldown. Stephen suggested replacing the current varnish bonding with a spring clamp, like what holds the workpiece RTD in place. 

I switched off the cryo cooler at 12pm today (Tue), so the chamber should be ready for venting Thursday or Friday. The tentative agenda is to add the spring clamp to secure the cold head RTD and cool down again (we will discuss any additional tweaks). I think I have an idea of why the current model predicts a much smaller time constant than we are seeing - I plan to work on this more this week. Hopefully once the cold head RTD stays fixed for an entire cooldown, this data can help tweak the model as well.

  2598   Fri Jul 2 11:27:01 2021 RadhikaDailyProgressCryo vacuum chamberCcooling updates 6/29-7/2

[Radhika, Stephen]

On Tuesday 6/29, we opened up Megastat after a weekend of warmup. Our goals were to 1) check on the RTD attached(?) to the cold plate to confirm that it had de-bonded, and 2) to check on the foil and mylar inside the chamber and around the copper braid. 

Indeed the tip of the cold head RTD had detached [attachment 1], but the mylar "cap" I created for insulation held up well. Inside the chamber, we noticed some shorting between aluminum foil on the inside of the outer lid and the outside of the inner lid [attachment 2]. Also, there was a gap in mylar around the copper braid, so some of the braid was visible. We also noticed that the strip of peek sheet inside the opening of the inner shield had slipped out of place, exposing the copper braid to the aluminum [attachment 8]. 

We rebonded the loose RTD to the cold head [attachment 3] and re-inserted the mylar "cap" [attachment 4 and 10]. Stephen suggested we add an additional piece of mylar to cover the portion of the cold head directly above the braid [attachment 5]. 

To prevent shorting inside the chamber, we trimmed the excess aluminum foil wrapped around the non-coated sides of the inner and outer shields [attachment 6]. We adjusted the mylar sheets around the copper braid to cover the previous gap, and used a mirror to ensure the bottom of the braid was covered [attachment 7]. We also realigned the peek sheet strip with the opening of the inner shield [attachment 9]. 

We reattached the heater to the workpiece [attachment 11] and the workpiece RTD with the spring clamp [attachment 12]. We placed back the inner and outer shield lids [attachment 13-14], closed up the chamber, and pumped down. Since I have been working on remotely extracting temperature data from the CTC-100, we chose to wait until the script was ready before turning on the cryocooler.

On Thursday 7/1, I got the temperature extraction script ready and turned on the cryocooler at ~5:15 PM. Fun addition: attachment 15 shows successful communication to the CTC-100 (I sent a command to display "hello" on the screen :D)

On Friday 7/2, I plotted the temperature trends so far [attachment 16]. As of 12pm Friday, the workpiece is at 177K. We will let the chamber cool over the weekend and see where we are on Tuesday.

 

  2597   Tue Jun 29 17:29:16 2021 StephenThings to Buy2um PhotodiodesIntegrating 2um PD measurements into Cryo Vacuum Chamber

Radhika and I started discussing in detail the items needed to transfer the 2um PD setup into the Cryo Vacuum Chamber.

1) Electrical

To interface with the PD setup, it seems that we will need want to use the feedthrough already in use on the IRLabs cryostat. This square-flanged feedthrough appears to host the in-vacuum cabling. The in-air cabling would ideally also be reused.

To implement this, we will need to modify a blank 2.75" conflat flange (in hand in QIL boxes on wire shelf) with a the following features:

  • through bore, 1.18 diameter on center.
  • a 4x #4-40 tapped hole square bolt pattern, 1.062" spacing on center.
  • preferably, a hand-polished o-ring sealing area.

I will take care of this part through the PMA shop.

2) Optical

The Cryo Vacuum Chamber windows are Thorlabs VPCHW42‐C (ref. D2000310-v1). The broadband AR coating is rated for 1050-1700 nm (here's the data sheet), with a steep climb in AR coating reflectance. There is also fused silica substrate transmission to worry about. Perhaps the easiest way to proceed would be to repeat Koji's Transmission test (ref. QIL/2458) for the windows already in use on the Cryo Vacuum Chamber, and see if we can accept ~10% loss (or more).

Else, perhaps we scavange the IRLabs cryostat and create another custom blank CF modification?

Or buy a new, suitable window with CF interface? (<---- preferred option)

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