40m QIL Cryo_Lab CTN SUS_Lab TCS_Lab OMC_Lab CRIME_Lab FEA ENG_Labs OptContFac Mariner WBEEShop
  Mariner elog  Not logged in ELOG logo
Message ID: 73     Entry time: Thu Aug 4 13:44:56 2022
Author: Jennifer Hritz 
Type: General 
Category: Optical Contacting 
Subject: Success with slowly heating 

Yesterday, I did two rounds of slowly heating 4 samples to the maximum hot plate temperature. This was to formally test if my success with a single sample earlier in the week was a fluke. Note that the hot plate takes about 10-15 minutes to reach a stable temperature when it is turned up one notch.

First round:
I bonded 4 samples by putting methanol in the gap between the glass slides and letting it dry to create a gap.
Starting at room temperature, I heated the slides on each setting for roughly 15 minutes, then let them cool down naturally over the course of an hour. 3 broke broke at medium heat, and 1 survived the whole process. I belive these broke because the bonds were weaker and I heated them slightly too quickly. In previous tests, I would manually switch the hot plate on and off, but I wanted to see if the hot plate could heat up slow enough on its own.

Second round:
I bonded 4 samples by scrubbing the slides with methanol, using a compressed air duster to blow off the fibers, rubbing them together with the pressure of my fingers, and repeating this whole procedure until they stuck (it took 2-4 repeats).
Starting at room temperature, I heated the slides on each setting for exactly 20 minutes, then let them cool down naturally over the course of an hour. All of them survived to the maximum temperature (the pictures show them at the start and end of the heating, note the temperature). I credit this to the stronger bonding proceedure and the extra 5 minutes for them to adjust to the temperature. I did not turn the hot plate on or off at any point, I just let it heat up at its own rate.

I cannot tell if the bonds are stronger. The size and shape of the Newtons rings did not change.

Attachment 1: PXL_20220803_232203193.jpg  2.433 MB  Uploaded Thu Aug 4 15:32:52 2022  | Hide | Hide all
Attachment 2: PXL_20220804_002433906.jpg  2.508 MB  Uploaded Thu Aug 4 15:32:57 2022  | Hide | Hide all
ELOG V3.1.3-