40m QIL Cryo_Lab CTN SUS_Lab TCS_Lab OMC_Lab CRIME_Lab FEA ENG_Labs OptContFac Mariner WBEEShop
  OMC elog  Not logged in ELOG logo
Message ID: 62     Entry time: Thu Feb 7 23:01:45 2013
Author: Koji 
Type: Optics 
Category: Characterization 
Subject: UV epoxy gluing test 

 [Jeff, Yuta, Koji]

Gluing test with UV-cure epoxy Optocast 3553-LV-UTF-HM

- This glue was bought in the end of October (~3.5 months ago).

- The glue was taken out from the freezer at 1:20pm.
- Al sheet was laid on the optical table. We made a boat with Al foil and pour the glue in it (@1:57pm)
- We brought two kinds of Cu wires from the 40m. The thicker one has the diameter of 1.62mm.
The thinner one has the diameter of 0.62mm. We decided to use thinner one being cut into 50mm in length.

- The OMC glass prisms have the footprint of 10mmx20mm = 200mm^2. We tested several combinations
of the substrates. Pairs of mirrors with 1/2" mm in dia. (127mm) and a pair of mirrors with 20mm in dia. (314mm).

- Firstly, a pair of 1/2" mirrors made of SF2 glass was used. A small dub on a thinner Cu wire was deposited on a mirror.
  We illuminated the glue for ~10sec. When the surfaces of the pair was matched, the glue did not spread on the entire
  surface. The glue was entirely spread once the pressure is applied by a finger. Glue was cured at 2:15pm. 12.873mm
  thickness after the gluing.

Some remark:
1. We should be careful not to shine the glue pot by the UV illuminator.
2. The gluing surface should be drag wiped to remove dusts on the surface.

- Secondly, we moved onto 20mm mirror pair taken from the remnant of the previous gluing test by the eLIGO people.
This time about 1.5 times more glue was applied.

- The third trial is to insert small piece of alminum foil to form a wedge. The thickness of the foil is 0.041mm.
The glue was applied to the pair of SF2 mirror (1/2" in dia.). A small dub (~1mm in dia) of the glue was applied.
The glue filled the wedge without any bubble although the glue tried to slide out the foil piece from the wedge.
So the handling was a bit difficult. After the gluing we measured the thickness of the wedge by a micrometer gauge.
The skinny side was 12.837mm, and the thicker side was 12.885mm. This is to be compared with the total thickness
12.823mm before the gluing. The wedge angle is 3.8mrad (0.22deg). The glue dub was applied at 2:43, and the UV
illumination was applied at 2:46.

- At the end we glued a pair of fused silica mirrors. The total thickness before the gluing was 12.658 mm.
The glue was applied at 2:59pm. The thickness after the gluing is 12.663 mm.
This indicates the glue thickess is 5um.

ELOG V3.1.3-