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Message ID: 367     Entry time: Tue May 28 12:14:20 2019
Author: Stephen 
Type: Optics 
Category: General 
Subject: CM PZT Assembly Debonding of EP30-2 in Acetone 

[LiyuanZ, StephenA]

Downs B119

Summary: Beginning on 20 May 2019, two CM PZT assemblies were soaked in Acetone in an effort to debond the EP30-2 bonds between tombstone-PZT and between PZT-optic. Debonding was straightforward after 8 days of soaking. 24 hours of additional acetone soaking will now be conducted in an attempt to remove remnant EP30-2 from bonding surfaces.

Procedure: The assemblies were allowed to soak in acetone for 8 days, with acetone level below the HR surface of the optic. No agitation of the solution, mechanical abrasion of the bond, or other disturbance was needed for the bond to soften.

GariLynn contributed the glassware and fume hood, and advised on the process (similar to debonding of CM and PZT from OMC SN002 after damaging event). The equipment list was (WIP, more detail / part numbers will be gathered today and tomorrow):

  • crystallizing dish (no spout, like a deep petri dish)
  • curved lid
  • wax sheet (to seal)
  • acetone
  • fume hood

Results: Today, 28 May 2019, I went to the lab to check on the optics after 8 days of soaking. Liyuan had monitored the acetone level during the first 4 days, topping up once on 24 May. All bonds were fully submerged for 8 days.

There were 2 assemblies soaked in one crystallizing dish. Debonded assemblies - ref OMC eLOG 328 for specified orientations and components:

PZT Assy #9 - ref. OMC eLOG 334 - M17+PZT#12+C10

PZT Assy #7 - ref. OMC eLOG 332 - M1+PZT#13+C13

PZT Assy #7 was investigated first.

  • C13 was removed with no force required.
  • PZT#13 was removed with no force required.
  • EP30-2 remained at the bond surfaces and tracing the diameters of each bond on each of the 3 bonding surfaces of the PZT and tombstone - these components were returned to the dish to soak.
  • No EP30-2 remained on the surface of the curved mirror - C13 was removed and stored.

A video of removal of C10 and PZT#12 from PZT Assy #9 was collected (See Attachment 8), showing the ease with which the debonded components could be separated.

  • C10 was removed with no force required.
  • A slight force - applied by gripping the barrel of the PZT and pushing with the index finger on the surface of the tombstone - was required to separate PZT#12 from M17,
    • likely due to excess glue at the barrel of the PZT
  • EP30-2 remained at the bond surfaces and tracing the diameters of each bond on each of the 3 bonding surfaces of the PZT and tombstone - these components were returned to the dish to soak.
  • No EP30-2 remained on the surface of the curved mirror - C13 was removed and stored.

Photos and video have been be added to supplement this report (edit 2019/07/08).

 

Attachment 1: omc367_IMG_3499_omc_removal_c13_from_CM7.JPG  2.758 MB  Uploaded Mon Jul 8 17:18:42 2019  | Show | Hide all | Show all
Attachment 2: omc367_IMG_3500_omc_removal_pzt13_from_CM7.JPG  2.490 MB  Uploaded Mon Jul 8 17:18:57 2019  | Hide | Hide all | Show all
omc367_IMG_3500_omc_removal_pzt13_from_CM7.JPG
Attachment 3: omc367_IMG_3501_omc_removal_pzt13_from_CM7_thickness.JPG  2.583 MB  Uploaded Mon Jul 8 17:19:12 2019  | Hide | Hide all | Show all
omc367_IMG_3501_omc_removal_pzt13_from_CM7_thickness.JPG
Attachment 4: omc367_IMG_3505_omc_removal_M1_from_CM7.JPG  2.328 MB  Uploaded Mon Jul 8 17:19:32 2019  | Hide | Hide all | Show all
omc367_IMG_3505_omc_removal_M1_from_CM7.JPG
Attachment 5: omc367_IMG_3507_omc_removal_c10_from_CM9.JPG  1.960 MB  Uploaded Mon Jul 8 17:19:36 2019  | Hide | Hide all | Show all
omc367_IMG_3507_omc_removal_c10_from_CM9.JPG
Attachment 6: omc367_IMG_3512_omc_removal_pzt12_from_CM9.JPG  2.273 MB  Uploaded Mon Jul 8 17:19:40 2019  | Show | Hide all | Show all
Attachment 7: omc367_IMG_3515_omc_removal_m17_from_CM9.JPG  2.274 MB  Uploaded Mon Jul 8 17:19:56 2019  | Hide | Hide all | Show all
omc367_IMG_3515_omc_removal_m17_from_CM9.JPG
Attachment 8: omc367_IMG_3506_omc_removal_of_c10_and_pzt12_from_CM9.MOV  79.996 MB  Uploaded Mon Jul 8 17:20:06 2019
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